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- Academic unit or major
- Chemistry
- Instructor(s)
- Ohmori Ken Kudo Fumitaka Takaya Jun Ando Yoshio Sase Shohei Miyanaga Akimasa
- Class Format
- Exercise
- Media-enhanced courses
- Day/Period(Room No.)
- Intensive ()
- Group
- -
- Course number
- ZSD.A433
- Credits
- 1
- Academic year
- 2018
- Offered quarter
- 1-2Q
- Syllabus updated
- 2018/3/20
- Lecture notes updated
- -
- Language used
- Japanese
- Access Index
-
Course description and aims
In this course, students operate instruments for mass spectrometry and NMR to determine the structures of organic molecules. Then, students attempt to solve the structure of the target molecules based on the mass and NMR data. The lecturers teach how to operate these instruments and how to analyze the obtained data. We discuss about the strategy for structural determination of organic molecules.
Nowadays, mass and NMR (including 2D NMR) analysis are widely taken for structural determination of relatively small organic molecules. Students will be able to take such spectra by themself and analyze the data for structural determination.
Student learning outcomes
By the end of this course, students will be able to:
1) Determine the structure of relatively small organic molecules.
2) Operate instruments for mass and NMR by themself
3) Analyze mass spectra and NMR spectra including 2D NMR data for structural determination
Keywords
Structural analysis of organic molecules, structure determination, mass spectral analysis, NMR, 2D-NMR
Competencies that will be developed
| ✔ Specialist skills | Intercultural skills | Communication skills | Critical thinking skills | ✔ Practical and/or problem-solving skills |
Class flow
In the first half of the class, we will discuss about previous spectral analysis taken by students. In the latter half, the lecturer teaches a main topic according to the course schedule. Students analyze mass spec and NMRs outside of the classroom.
Course schedule/Required learning
| Course schedule | Required learning | |
|---|---|---|
| Class 1 | Introduction to structural analysis of organic compounds | Decide a target sample for analysis |
| Class 2 | Mass spectral analysis of organic compounds | Mass spectral analysis and make a report |
| Class 3 | 1H-NMR | 1H-NMR analysis and make a report |
| Class 4 | 13C-NMR | 13C-NMR analysis and make a report |
| Class 5 | COSY | COSY analysis and make a report |
| Class 6 | HMQC, HMBC | HMQC, HMBC analysis and make a report |
| Class 7 | NOE | NOE analysis and make a report |
| Class 8 | Structural determination of organic compounds | Final report |
Textbook(s)
Course materials are provided during class.
Reference books, course materials, etc.
Spectrometric Identification of Organic Compounds
Assessment criteria and methods
Exercise problems in each class (60%) and a final report (40%)
Related courses
- Practical Exercises for Advanced Instrumental Measurements I
- ZSD.A433 ： Practical Exercises for Advanced Instrumental Measurements III
- Structural Organic Chemistry
Prerequisites (i.e., required knowledge, skills, courses, etc.)
No prerequisites are necessary. But, students who have a credit for Practical Exercises for Advanced Instrumental Measurements I or Practical Exercises for Advanced Instrumental Measurements II, cannot take this class.
Contact information (e-mail and phone) Notice : Please replace from "[at]" to "@"(half-width character).
Fumitaka Kudo: fkudo[at]chem.titech.ac.jp
Office hours
Students may approach the instructors at the end of class or contact by e-mail in advance to schedule an appointment.
